ORGANIC CHEMISTRY 3510

TENTATIVE SYLLABUS

DR. SUNDIN

FALL, 2005

Ottensman 317

The experiments are from Microscale Organic Laboratory, 4th Ed.; Mayo, Pike, and Trumper; Wiley; 2000.

WEEK OF, EXPERIMENT, PAGES

September 6, 7, 12: Introduction, The Notebook, Check In; pages 1-17, 29-32.
September 12, 13, 14: Melting Point, Unknown Solid, Experiment 1(a); pages 33-34, 40, 42-43, 99-103.
September 19, 20, 21: Infrared Spectroscopy, Unknown Liquid, Experiment 1(c); pages 104-105, 534-535, 544-547.
September 26, 27, 28: Dehydration, Gas Chromatography Analysis, Experiment 9; pages 16-24, 27-28, 44-48, 184-192; "Abstract".
October 3, 4, 5: Boiling Point, Refractive Index, Unknown Liquid, Experiment 1(b); pages 34-36, 38-40.
October 10, 11, 12: Extraction, Partition Coefficient, Experiments 4A, 4B; pages 26-27, 29, 55-63, 67-69, 123-129; "Discussion".
October 17, 18, 19: Extraction, Separation of a Mixture, Experiment 4C; pages 65-66, 129-132; "Experimental".
October 24, 25, 26: Simple Distillation, Experiment 3A; pages 22-23, 50-52, 112-115, 554-558, 573-574, 581-582.
October 26: EXAM 1; Wednesday, 7:00-9:00 pm, Ottensman 103 and 105.
October 31, November 1, 2: Reduction, Experiment 5B; pages 133-135, 139-144.
November 7, 8, 9: Finish Reduction and Gas Chromatography Analysis; "Total".
November 14, 15, 16: Recrystallization, Set Up Photoisomerization, Experiment 6A; pages 71-75, 145-149.
November 21, 22, 23: Craig Tube Recrystallization; Experiment 6B; pages 75-77, 149.
November 28, 29, 30: Isolation of a Natural Product, Sublimation, Caffeine in Tea, Experiment 11B; pages 87-88, 96-98, 199, 204-209.
December 5, 6, 7: Carbohydrates, Proteins and Amino Acid.
December 12, 13, 14: High Performance Liquid Chromatography, Quantitative Determination of Caffeine in a Beverage; pages 85-86; Clean Up; Check Out.

December 21: EXAM 2; Wednesday, 8:00-9:52 am.